Matrix solid-phase dispersion extraction of organophosphorus pesticide using SiO2-poly(N-vinylimidazole)
نویسندگان
چکیده
منابع مشابه
Solid-phase extraction and cleanup of organophosphorus pesticide residues in bovine muscle with gas chromatographic detection.
The purpose of this investigation is to develop a rapid and simple method for the assessment of organophosphorus pesticides in bovine muscle by using solid-phase extraction (SPE). After extraction with ethyl acetate (EtOAc) the homogenate is centrifuged and filtered through sodium sulfate. The fat is precipitated in methanol by cooling and the extract is diluted with water and passed through a ...
متن کاملMatrix solid phase dispersion (MSPD).
A review of the many uses of matrix solid phase dispersion (MSPD) in the extraction and analysis of a variety of compounds from a range of samples is provided. Matrix solid phase dispersion (MSPD) has found particular application as a somewhat generic analytical process for the preparation, extraction and fractionation of solid, semi-solid and/or highly viscous biological samples. Its simplicit...
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The aim of this work was to optimize an analytical method to determine residues of 21 organophosphorus pesticides of different polarities in drinking water using graphitized carbon black extraction cartridges liquid-solid and gas chromatography. The extraction was performed passing 100 mL of sample at 5 mL/min through 250 mg black graphitized carbon previously conditioned. The elution was carri...
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Phosalone, malathion and diazinon were analyzed in corn oil using solid phase extraction (SPE)with lanthanum silicate as a new solid sorbent followed by gas chromatography with nitrogenphosphorus detection (GC-NPD). The efficiency of different eluents (methanol, dichloromethane,ethyl acetate, dichloromethane — ethyl acetate (1:1) and ethyl acetate — methanol (1:1)) werecompared for elution of o...
متن کاملDetermination of Malathion and α-Endosulfan Residue in Khazar Rice Using Matrix Solid Phase Dispersion and HPLC
An extraction method based on matrix solid phase dispersion (MSPD) and high performance liquid chromatography with UV detection for quantification of two widely used pesticides (Malathion and α-Endosulfan) in Khazar rice from north of Iran were investigated. The ratio of solid phase (adsorbent) to sample, types of eluting solvent and its volume were optimized to achieve the highest recoveries f...
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ژورنال
عنوان ژورنال: IOP Conference Series: Materials Science and Engineering
سال: 2013
ISSN: 1757-8981,1757-899X
DOI: 10.1088/1757-899x/45/1/012022